chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester
CAS No.:1015181-15-3
Molecular Formula:C₅₉H₅₅ClN₂O₁₅
Molecular Weight:1067.54
Hs Code.:

chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

Synonyms:chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

Suppliers and Price of chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

There total 1 articles about chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2-[4-benzyloxy-5-hydroxy-2-methoxy-6-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

: 560129-48-8
ethyl 3,6-di-O-benzyl-4-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1015181-15-3
chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

Guidance literature:: With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; at -20 ℃;
DOI:10.1016/j.mencom.2007.01.004

Reference yield: 93.0%

: 1015181-15-3
chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

: 1015181-25-5
chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-hydroxymethyl-6-methoxy-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; at 0 ℃;
DOI:10.1016/j.mencom.2007.01.004

Reference yield:

: 1015181-15-3
chloro-acetic acid 4-benzyloxy-6-[4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-6-methoxy-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yloxy]-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yl ester

: 1015180-91-2
C₆₇H₇₀N₂O₁₉

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / ammonium cerium(IV) nitrate / H₂O; acetonitrile / 0 °C

2: 77 percent / CuBr₂; Bu₄NBr / CH₂Cl₂; dimethylformamide / 20 °C

3: 95 percent / water / pyridine / 80 °C

With ammonium cerium(IV) nitrate; tetrabutylammomium bromide; water; copper(ll) bromide; In pyridine; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.mencom.2007.01.004