benzyl 6-O-t-butyldimethylsilyl-4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

Base Information

Chemical Name:benzyl 6-O-t-butyldimethylsilyl-4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside
CAS No.:1192256-54-4
Molecular Formula:C₂₃H₃₄O₄Si
Molecular Weight:402.606
Hs Code.:

Synonyms:benzyl 6-O-t-butyldimethylsilyl-4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

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Chemical Property of benzyl 6-O-t-butyldimethylsilyl-4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

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Technology Process of benzyl 6-O-t-butyldimethylsilyl-4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

There total 1 articles about benzyl 6-O-t-butyldimethylsilyl-4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 81389-87-9
(2R,3S,6S)-6-(benzyloxy)-2-(((tert-butyldimethylsilyl)oxy)methyl)-3,6-dihydro-2H-pyran-3-ol

: 3355-28-0
1-Bromo-2-butyne

: 1192256-54-4
benzyl 6-O-t-butyldimethylsilyl-4-O-(2-butynyl)-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

Guidance literature:: (2R,3S,6S)-6-(benzyloxy)-2-(((tert-butyldimethylsilyl)oxy)methyl)-3,6-dihydro-2H-pyran-3-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.0833333h; Reflux;

1-Bromo-2-butyne; In tetrahydrofuran; mineral oil; for 18h; Reflux;
DOI:10.1016/j.tet.2009.07.088