(-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate

Base Information

Chemical Name:(-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate
CAS No.:77059-69-9
Molecular Formula:CH₂Cl₂*C₄₀H₄₀ClNiP₄*F₆P
Molecular Weight:968.693
Hs Code.:

(-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate

Synonyms:(-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate

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Chemical Property of (-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate

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Technology Process of (-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate

There total 1 articles about (-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: ammonium hexafluorophosphate

: 72091-01-1,72091-02-2,72150-36-8,72150-63-1,77410-05-0
(S,S)-1,2-bis(methylphenylphosphino)benzene

: 87760-26-7,77029-28-8
{T-4-(R(*),S(*))}-dicarbonyl{1,2-phenylenebis(methylphenylphosphine)}nickel⁽⁰⁾

: 77059-69-9
(-)-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR)-o-phenylenebis(methylphenylphosphine))nickel(II) hexafluorophosphate dichloromethane solvate

Guidance literature:: With sulfuryl dichloride; In ethanol; dichloromethane; water; byproducts: CO, SO2; dicarbinyl dissolved in dichloromethane and soln. treated with SO2Cl2 in dichloromethane at 0°C under N2 atm., after 20 min (SS)-diphos added, solvent removed and residue dissolved in ethanol, NH4PF6 in wateradded; ppt. washed and dried and recrystd. from dichloromethane by addn. diethyl ether; elem. anal.;