diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate

Base Information

Chemical Name:diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate
CAS No.:1289220-75-2
Molecular Formula:C₁₄H₁₈F₂N₃O₄P
Molecular Weight:361.285
Hs Code.:

Synonyms:diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate

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Technology Process of diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate

There total 2 articles about diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1289220-59-2
diethyl 2-azido-1-hydroxyethylphosphonate

: 302912-34-1
2,4-difluoroethynylbenzene

: 1289220-75-2
diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1080/10426507.2010.494646

Reference yield:

: 20030-44-8
epoxy-1,2 ethyl phosphonate de diethyle

: 1289220-75-2
diethyl 2-[4-(2,4-difluorophenyl)-1,2,3-triazol-1-yl]-1-hydroxyethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium sulfate; sodium azide / methanol / 4 h / 65 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C

With ammonium sulfate; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In methanol; water; tert-butyl alcohol;
DOI:10.1080/10426507.2010.494646