(1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]

Base Information

Chemical Name:(1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]
CAS No.:384344-40-5
Molecular Formula:C₂₄H₄₀O₆
Molecular Weight:424.578
Hs Code.:

(1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]

Synonyms:(1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]

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Chemical Property of (1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]

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Technology Process of (1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]

There total 1 articles about (1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

: 133887-41-9
(1R*,4aS*,4bR*,8aR*,10aS*)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetra-methyl-trans-anti-trans-phenanthene-2(1H)-one

: 384344-33-6
(1R,4aS,4bR,8aR,10aS)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]

: 384344-40-5
(1S,4aR,4bS,8aS,10aR)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetramethyl-trans-anti-trans-phenanthrene-2(1H)-one-2-[((1S,2S)-di(hydroxymethyl))ethylene acetal]

Guidance literature:: (2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol; (1R*,4aS*,4bR*,8aR*,10aS*)-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-1-methoxycarbonyl-4b,8,8,10a-tetra-methyl-trans-anti-trans-phenanthene-2(1H)-one; With toluene-4-sulfonic acid; In benzene; for 2h; Heating;

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 48h;
DOI:10.1016/S0040-4020(01)00825-0