4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,0^2,90^3,70^6,8>tetradeca-4,13-dien-11,12-dicarboxylate

Base Information

• Chemical Name: 4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,0^2,90^3,70^6,8>tetradeca-4,13-dien-11,12-dicarboxylate
• CAS No.: 73249-36-2
• Molecular Formula: C₄₂H₃₈N₂O₄
• Molecular Weight: 634.775

Synonyms:4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,0^2,90^3,70^6,8>tetradeca-4,13-dien-11,12-dicarboxylate

Chemical Property of 4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,0^2,90^3,70^6,8>tetradeca-4,13-dien-11,12-dicarboxylate

Chemical Property:

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Technology Process of 4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,0^2,90^3,70^6,8>tetradeca-4,13-dien-11,12-dicarboxylate

There total 2 articles about 4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,0^2,90^3,70^6,8>tetradeca-4,13-dien-11,12-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

endo-exo-diethyl 4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,14,702,903,8>pentadeca-5,13-dien-15-one-11,12-dicarboxylate (73240-58-1) → 4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,02,903,706,8>tetradeca-4,13-dien-11,12-dicarboxylate (73249-36-2)

Guidance literature:

at 210 ℃;

DOI:10.1016/0040-4020(80)88028-8

Reference yield:

→ 1,2,2a,6c-tetraphenyl-2a,2b,2c,3,6,6a,6b,6c-octahydro-3,6-etheno-cyclopropa[3,4]pentaleno[1,2-d]pyridazine-4,5-dicarboxylic acid diethyl ester (73249-36-2)

Guidance literature:

Tetracyclon-Addukt 7, Δ;

DOI:10.1016/S0040-4039(01)86394-2

Reference yield: 64.0%

4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,02,903,706,8>tetradeca-4,13-dien-11,12-dicarboxylate (73249-36-2) → cis-exo-9,10,11,12-tetraphenyltetracyclo<6,3,1,02,709,12>dodeca-3,5,10-triene (73240-63-8)

Guidance literature:

With potassium hydroxide; In ethanol; Heating;

DOI:10.1016/0040-4020(80)88028-8

upstream raw materials:

endo-exo-diethyl 4,5,6,7-tetraphenyl-11,12-diazapentacyclo<8,2,2,1^4,70^2,90^3,8>pentadeca-5,13-dien-15-one-11,12-dicarboxylate

Downstream raw materials:

cis-exo-9,10,11,12-tetraphenyltetracyclo<6,3,1,0^2,70^9,12>dodeca-3,5,10-triene

C₄₀H₃₀O₃

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