Fe(OH)[(C₄H₂NC(C₆H₄NHCOC(CH₃)3))2(C₄H₂NC(C₆H₄NHCOC₆H₄NC(CH₃)NCH₂))2]

Base Information

• Chemical Name: Fe(OH)[(C₄H₂NC(C₆H₄NHCOC(CH₃)3))2(C₄H₂NC(C₆H₄NHCOC₆H₄NC(CH₃)NCH₂))2]
• CAS No.: 104070-12-4
• Molecular Formula: C₇₄H₆₅FeN₁₂O₅
• Molecular Weight: 1258.25
• Mol file: 104070-12-4.mol

Synonyms:Fe(OH)[(C₄H₂NC(C₆H₄NHCOC(CH₃)3))2(C₄H₂NC(C₆H₄NHCOC₆H₄NC(CH₃)NCH₂))2]

Chemical Property of Fe(OH)[(C₄H₂NC(C₆H₄NHCOC(CH₃)3))2(C₄H₂NC(C₆H₄NHCOC₆H₄NC(CH₃)NCH₂))2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Fe(OH)[(C₄H₂NC(C₆H₄NHCOC(CH₃)3))2(C₄H₂NC(C₆H₄NHCOC₆H₄NC(CH₃)NCH₂))2]

There total 1 articles about Fe(OH)[(C₄H₂NC(C₆H₄NHCOC(CH₃)3))2(C₄H₂NC(C₆H₄NHCOC₆H₄NC(CH₃)NCH₂))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

[(C4H2NHC(C6H4NHCOC(CH3)3))2(C4H2NC(C6H4NHCOC6H4NC(CH3)NCH2))2] (104070-03-3) + iron(II) bromide (7789-46-0) → Fe(OH)[(C4H2NC(C6H4NHCOC(CH3)3))2(C4H2NC(C6H4NHCOC6H4NC(CH3)NCH2))2] (104070-12-4) + Fe2O[(C4H2NC(C6H4NHCOC(CH3)3))2(C4H2NC(C6H4NHCOC6H4NC(CH3)NCH2))2]2*4H2O

Guidance literature:

With K₂CO₃; In tetrahydrofuran; benzene; excess of FeBr2, stirred at room temp. overnight (anaerobic conditions); aerobic workup; solvents removed, residue extd. with CH2Cl2, concd., washed with aq. HBr, H2O, concd. NH4OH, H2O, aq. sodium citrate, H2O, CH2Cl2 soln. dried over Na2SO4, heptane added, chromd. (silica gel, CHCl3/ether/methanol=30:5:1), elem. anal.;

DOI:10.1021/ja00282a020

upstream raw materials:

[(C₄H₂NHC(C₆H₄NHCOC(CH₃)3))2(C₄H₂NC(C₆H₄NHCOC₆H₄NC(CH₃)NCH₂))2]

iron(II) bromide