dicarbonyl{3-5-η-1-σ-2-cyano-1-(methoxycarbonyl)cyclohept-3-enediyl}(triphenyl phosphite)iron

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Chemical Name:dicarbonyl{3-5-η-1-σ-2-cyano-1-(methoxycarbonyl)cyclohept-3-enediyl}(triphenyl phosphite)iron
CAS No.:137203-89-5
Molecular Formula:C₃₀H₂₆FeNO₇P
Molecular Weight:599.36
Hs Code.:

Synonyms:dicarbonyl{3-5-η-1-σ-2-cyano-1-(methoxycarbonyl)cyclohept-3-enediyl}(triphenyl phosphite)iron

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Chemical Property of dicarbonyl{3-5-η-1-σ-2-cyano-1-(methoxycarbonyl)cyclohept-3-enediyl}(triphenyl phosphite)iron

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Technology Process of dicarbonyl{3-5-η-1-σ-2-cyano-1-(methoxycarbonyl)cyclohept-3-enediyl}(triphenyl phosphite)iron

There total 1 articles about dicarbonyl{3-5-η-1-σ-2-cyano-1-(methoxycarbonyl)cyclohept-3-enediyl}(triphenyl phosphite)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 137203-94-2
dicarbonyl{1-5-η-1-(methoxycarbonyl)cyclohepta-1,3-dienylium}(triphenyl phosphite)iron hexafluorophosphate

: 137203-89-5
dicarbonyl{3-5-η-1-σ-2-cyano-1-(methoxycarbonyl)cyclohept-3-enediyl}(triphenyl phosphite)iron

Guidance literature:: With KCN; In acetonitrile; (Ar or N2); addn. of KCN to soln. of Fe complex, 0°C, stirring, 20 min; warming to room temp., partitioned between H2O and Et2O, sepg. layers, extg. aq. phase twice with Et2O, washing with brine, drying (MgSO4), removal of solvent in vac., flash chromy. (SiO2, 30% EtOAc/hexanes);
DOI:10.1021/om00037a072