N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine

Base Information

Chemical Name:N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine
CAS No.:937021-55-1
Molecular Formula:C₁₇H₂₅FN₂O₂
Molecular Weight:308.396
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine

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Chemical Property of N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine

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Technology Process of N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine

There total 3 articles about N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 843651-80-9
N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]hydrazine

: 937021-55-1
N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm050538l

Reference yield:

: 350-40-3
2-(4-fluorophenyl)-1-propene

: 937021-55-1
N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: NBS / CCl₄ / Heating

2: 24 percent / NEt₃ / methanol / 3 h / Heating

3: 66 percent / N,N-diisopropylethylamine / dimethylformamide / 20 °C

With N-Bromosuccinimide; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050538l

Reference yield:

: 132927-05-0
1-(3-bromoprop-1-en-2-yl)-4-fluorobenzene

: 937021-55-1
N-tert-butoxycarbonyl-N'-[2-(4-fluorophenyl)allyl]-N'-isopropylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / NEt₃ / methanol / 3 h / Heating

2: 66 percent / N,N-diisopropylethylamine / dimethylformamide / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm050538l