4-FLUORO-2-TRIFLUOROMETHOXY-BENZOIC ACID HYDRAZIDE

Base Information

• Chemical Name: 4-FLUORO-2-TRIFLUOROMETHOXY-BENZOIC ACID HYDRAZIDE
• CAS No.: 887596-89-6
• Molecular Formula: C₈H₆F₄N₂O₂
• Molecular Weight: 238.141
• Mol file: 887596-89-6.mol

Synonyms:4-FLUORO-2-TRIFLUOROMETHOXY-BENZOIC ACID HYDRAZIDE

Chemical Property of 4-FLUORO-2-TRIFLUOROMETHOXY-BENZOIC ACID HYDRAZIDE

Chemical Property:

• PSA: 67.84000
• LogP: 2.60290

Purity/Quality:

99%+ ^*data from raw suppliers

4-Fluoro-2-trifluoromethoxy-benzoicacidhydrazide 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-FLUORO-2-TRIFLUOROMETHOXY-BENZOIC ACID HYDRAZIDE

There total 2 articles about 4-FLUORO-2-TRIFLUOROMETHOXY-BENZOIC ACID HYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

ethyl 4-fluoro-2-(trifluoromethoxy)benzoate → 4-fluoro-2-(trifluoromethoxy)benzohydrazide (887596-89-6)

Guidance literature:

With hydrazine hydrate; In tert-Amyl alcohol; at 80 ℃; for 24h;

Reference yield:

4-fluoro-2-(trifluoromethoxy)benzoic acid → 4-fluoro-2-(trifluoromethoxy)benzohydrazide (887596-89-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: thionyl chloride / 0.25 h / 20 °C

1.2: 2 h / 0 - 80 °C

2.1: hydrazine hydrate / tert-Amyl alcohol / 24 h / 80 °C

With thionyl chloride; hydrazine hydrate; In tert-Amyl alcohol;

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