benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester

Base Information

Chemical Name:benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester
CAS No.:1392506-45-4
Molecular Formula:C₃₆H₃₅N₃O₃
Molecular Weight:557.692
Hs Code.:

Synonyms:benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester

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Chemical Property of benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester

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Technology Process of benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester

There total 1 articles about benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 591-50-4
iodobenzene

: 1392506-36-3
tert-butyl (2-(diphenylmethylene)-1-(prop-2-yn-1-yl)hydrazine-1-carbonyl)-D-phenylalaninate

: 1392506-45-4
benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine; In N,N-dimethyl-formamide; for 12h; Inert atmosphere;
DOI:10.1021/ol302021n

Reference yield:

: 1392506-45-4
benzhydrylidene aza-phenylpropargylglycinyl-D-phenylalanine tert-butyl ester

: 1392506-46-5
(2'R,4Z)-1-((diphenylmethylene)amino)-3-(tert-butyl-3'-phenyl-2'-propanoate)-4-benzylidene-imidazolidin-2-one

: (2'S,4Z)-1-((diphenylmethylene)amino)-3-(tert-butyl-3'-phenyl-2'-propanoate)-4-benzylidene-imidazolidin-2-one

: C₃₆H₃₅N₃O₃

Guidance literature:: With sodium hydride; In acetonitrile; mineral oil; at 20 ℃; for 12h; Overall yield = 69%; Overall yield = 34.3 mg; Inert atmosphere;
DOI:10.1021/ol302021n