1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

Base Information

Chemical Name:1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone
CAS No.:1616629-03-8
Molecular Formula:C₁₇H₁₆N₄O₂
Molecular Weight:308.34
Hs Code.:

Synonyms:1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

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Chemical Property of 1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

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Technology Process of 1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

There total 3 articles about 1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1616629-01-6
1-[5-(2-methyl-5-nitrobenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

: 1616629-03-8
1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 24h; under 22502.3 Torr; Autoclave;

Reference yield:

: 1186502-34-0
1-(5-amino-1H-pyrrolo[2,3-b]pyridin-2-yl)-ethanone

: 1616629-03-8
1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 22502.3 Torr / Autoclave

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 1186502-33-9
C₉H₇N₃O₃

: 1616629-03-8
1-[5-(5-amino-2-methylbenzoylamino)-1H-pyrrolo[2,3-b]pyridin-2-yl]-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 26252.6 Torr

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 22502.3 Torr / Autoclave

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; N,N-dimethyl-formamide;