[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)

Base Information

Chemical Name:[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)
CAS No.:1240076-00-9
Molecular Formula:C₅₉H₆₄N₄SiZn
Molecular Weight:922.659
Hs Code.:

Synonyms:[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)

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Chemical Property of [5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)

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Technology Process of [5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)

There total 1 articles about [5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 444103-21-3
C₅₄H₅₅BrN₄Zn

: 1066-54-2
trimethylsilylacetylene

: 1240076-00-9
[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)

Guidance literature:: With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201100642

Reference yield: 94.0%

: 1240076-00-9
[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)

: 952190-20-4
[5,15-bis(3,5-di-tert-butylphenyl)-10-ethynyl-20-phenylporphyrinato]zinc(II)

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 20 ℃; for 0.333333h;
DOI:10.1002/ejoc.201100642

Reference yield: 71.0%

: 1240076-00-9
[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trimethylsilanylethynyl)porphyrinato]zinc(II)

: C₅₀H₇₀I₂N₂O₂

: C₁₀₆H₁₂₅IN₆O₂Zn

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; tetrabutyl ammonium fluoride; diisopropylamine; triphenylphosphine; In tetrahydrofuran; at 45 ℃; for 1h;
DOI:10.1021/acs.chemmater.5b02006