C₂₄H₃₀O₄

Base Information

Chemical Name:C₂₄H₃₀O₄
CAS No.:1264756-65-1
Molecular Formula:C₂₄H₃₀O₄
Molecular Weight:382.5
Hs Code.:

C<sub>24</sub>H<sub>30</sub>O<sub>4</sub>

Synonyms:C₂₄H₃₀O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₀O₄

Chemical Property:

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Technology Process of C₂₄H₃₀O₄

There total 13 articles about C₂₄H₃₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1264756-64-0
C₃₂H₃₈O₅

: 1264756-65-1
C₂₄H₃₀O₄

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-61-7
C₂₈H₃₄O₅

: 1264756-65-1
C₂₄H₃₀O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane / -78 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

4.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; dichloromethane; water; 1.1: Swern oxidation / 1.2: Wittig reaction / 3.1: Sharpless asymmetric epoxidation / 5.1: Wittig reaction;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-62-8
C₃₃H₄₀O₆

: 1264756-65-1
C₂₄H₃₀O₄

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / dichloromethane / -78 °C

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

3: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

4: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

5: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; dichloromethane; water; 2: Sharpless asymmetric epoxidation / 4: Wittig reaction;
DOI:10.1016/j.tetlet.2010.11.127