1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

Base Information

Chemical Name:1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine
CAS No.:886228-63-3
Molecular Formula:C₂₂H₃₇NO₂Si
Molecular Weight:375.627
Hs Code.:

1-[2-(<i>tert</i>-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

Synonyms:1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

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Chemical Property of 1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

Chemical Property:

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Technology Process of 1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

There total 7 articles about 1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methanesulfonic acid 2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl ester

: 63126-47-6,76946-27-5,84025-81-0,135523-48-7
(2R)-methoxymethylpyrrolidine

: 886228-63-3
1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

Guidance literature:: In dichloromethane; for 2h;
DOI:10.1055/s-2006-932489

Reference yield:

: 444020-03-5
2-formyloxymethyl-3-phenyl-acrylic acid methyl ester

: 886228-63-3
1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

Guidance literature:: Multi-step reaction with 5 steps

1: aq. HCl / methanol

2: 100 percent / imidazole / dimethylformamide

3: 86 percent / DIBAL-H / CH₂Cl₂

4: Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

5: 230 mg / CH₂Cl₂ / 2 h

With 1H-imidazole; hydrogenchloride; diisobutylaluminium hydride; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-932489

Reference yield:

: 444020-05-7
2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-acrylic acid methyl ester

: 886228-63-3
1-[2-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-allyl]-2-methoxymethyl-pyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / DIBAL-H / CH₂Cl₂

2: Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

3: 230 mg / CH₂Cl₂ / 2 h

With diisobutylaluminium hydride; triethylamine; In dichloromethane;
DOI:10.1055/s-2006-932489