6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester

Base Information

• Chemical Name: 6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester
• CAS No.: 191853-65-3
• Molecular Formula: C₆₈H₆₃N₇O₁₅
• Molecular Weight: 1218.29

Synonyms:6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester

Chemical Property of 6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of 6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester

There total 1 articles about 6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-methyl-3-p-nitrobenzyloxycarbonylimidazolium chloride + 6-((2R,3S,4R,5R)-4-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-3-yloxy)-hexanoic acid 9H-fluoren-9-ylmethyl ester (191853-61-9) → 6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester (191853-65-3)

Guidance literature:

With dmap; In dichloromethane; Ambient temperature;

DOI:10.1002/hlca.19970800313

Reference yield: 92.0%

6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester (191853-65-3) → 6-{(2R,3R,4R,5R)-2-Hydroxymethyl-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester (191853-69-7)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; chloroform; for 0.25h; Ambient temperature;

DOI:10.1002/hlca.19970800313

Reference yield: 87.0%

6-{(2R,3R,4R,5R)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester (191853-65-3) → 3'-deoxy-5'-O-[(4-methoxyphenyl)diphenylmethyl]-N6-[2-(4-nitrophenyl)ethoxycarbonyl]adenylyl-(2'-{OP-[2-(4-nitrophenyl)ethyl]} - 5')-3'-deoxy-N6-[2-(4-nitrophenyl)ethoxycarbonyl]adenylyl-(2'-{OP-[2-(4-nitrophenyl)ethyl]} - 5')-3'-O-...

Guidance literature:

With piperidine; In ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19970800313

upstream raw materials:

6-((2R,3S,4R,5R)-4-Hydroxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-tetrahydro-furan-3-yloxy)-hexanoic acid 9H-fluoren-9-ylmethyl ester

Downstream raw materials:

6-{(2R,3R,4R,5R)-2-Hydroxymethyl-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-3-yloxy}-hexanoic acid 9H-fluoren-9-ylmethyl ester

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