3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine

Base Information

• Chemical Name: 3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine
• CAS No.: 113297-69-1
• Molecular Formula: C₁₀₃H₈₁Cl₂N₁₅O₂₂P₂
• Molecular Weight: 2013.72

Synonyms:3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine

Chemical Property of 3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine

Chemical Property:

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Technology Process of 3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine

There total 1 articles about 3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3'-O-Benzoyladenylyl-<2'--5'>-N6,N6,2',3'-tetrabenzoyladenosine (113297-66-8) + Benzoic acid (2R,3R,4R,5R)-5-(6-amino-purin-9-yl)-4-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-2-trityloxymethyl-tetrahydro-furan-3-yl ester; compound with triethyl-amine (113297-63-5) → 3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N6,N6,2',3'-tetrabenzoyladenosine (113297-69-1)

Guidance literature:

With pyridine; 1-(2,4,6-triisopropylphenylsulfonyl)-1H-1,2,4-triazole; for 15h; Ambient temperature;

Reference yield: 60.0%

3'-O-Benzoyl-5'-O-trityladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N6,N6,2',3'-tetrabenzoyladenosine (113297-69-1) → 3'-O-Benzoyladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N6,N6,2',3'-tetrabenzoyladenosine (113297-70-4)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; Ambient temperature;

upstream raw materials:

3'-O-Benzoyladenylyl-<2'--5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine

Benzoic acid (2R,3R,4R,5R)-5-(6-amino-purin-9-yl)-4-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-2-trityloxymethyl-tetrahydro-furan-3-yl ester; compound with triethyl-amine

Downstream raw materials:

3'-O-Benzoyladenylyl-<2'--5'>-3'-O-benzoyladenylyl-<2'-5'>-N⁶,N⁶,2',3'-tetrabenzoyladenosine

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