methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

Base Information

Chemical Name:methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate
CAS No.:1350706-97-6
Molecular Formula:C₂₂H₂₃BrN₂O₄
Molecular Weight:459.34
Hs Code.:

Synonyms:methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

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Technology Process of methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

There total 1 articles about methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110-52-1
1,4-dibromo-butane

: 525601-46-1
methyl 2-(2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

: 1350706-97-6
methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

Guidance literature:: methyl 2-(2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate; With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetone; for 1h; Reflux;

1,4-dibromo-butane; In acetone; at 20 ℃; for 120h;
DOI:10.1016/j.ejmech.2011.09.032

Reference yield: 97.0%

: 136918-14-4,85-41-6
phthalimide

: 1350706-97-6
methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

: methyl 2-(3-(4-(1,3-dioxoisoindolin-2-yl)butyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

Guidance literature:: phthalimide; With tetrabutylammomium bromide; potassium carbonate; In acetone; at 60 ℃; for 0.5h;

methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate; In acetone; at 60 ℃; for 2h;
DOI:10.1016/j.ejmech.2011.09.032

Reference yield: 81.0%

: 1350706-97-6
methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate

: 5807-14-7,389623-48-7
1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine

: 2-(3-(4-(2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidin-1-yl)butyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetic acid hydrochloride

Guidance literature:: 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; With tetrabutylammomium bromide; potassium carbonate; In acetone; at 60 ℃; for 1h;

methyl 2-(3-(4-bromobutyl)-2,5-dioxo-4,4-diphenylimidazolidin-1-yl)acetate; In acetone; at 60 ℃;

With hydrogenchloride; In methanol; diethyl ether;
DOI:10.1016/j.ejmech.2011.09.032