(4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone

Base Information

Chemical Name:(4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone
CAS No.:262604-04-6
Molecular Formula:C₂₁H₃₀BNO₆
Molecular Weight:403.283
Hs Code.:

Synonyms:(4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone

There total 2 articles about (4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 262604-01-3
(4S)-3-t-butyloxycarbonyl-4-(4-iodobenzyl)-5-oxazolidinone

: 262604-04-6
(4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone

Guidance literature:: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 80 ℃; for 27h;
DOI:10.1246/bcsj.73.231

Reference yield: 71.0%

: bis(2,3-dimethyl-2,3-butanediolato)diboron

: 262604-01-3
(4S)-3-t-butyloxycarbonyl-4-(4-iodobenzyl)-5-oxazolidinone

: 262604-04-6
(4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone

Guidance literature:: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; under Ar; 80°C, 27 h; quenching (water), extn. (ether), column chromy. (SiO2, hexane/ethyl acetate = 5:1); elem. anal.;
DOI:10.1246/bcsj.73.231

Reference yield: 67.0%

: 7732-18-5
water

: 262604-04-6
(4S)-3-t-butyloxycarbonyl-4-[4-(2,3-dimethyl-2,3-butanediolatoboryl)benzyl]-5-oxazolidinone

: 76410-58-7
p-borono-L-phenylalanine

Guidance literature:: With sodium hydroxide; sodium periodate; sulfuric acid; In 1,4-dioxane; water; acetone; 1) NaIO4, NH4OAc, acetone/water, room temp., 48 h; 2) aq. NaOH, 1 h; 3)aq. H2SO4, 1,4-dioxane, room temp., 1 h; removal of solvent, neutralization with aq. NaOH;
DOI:10.1246/bcsj.73.231