1,1-Bis(4-bromophenyl)-2-(2,4,6-trinitrophenyl)hydrazine

Base Information

• Chemical Name: 1,1-Bis(4-bromophenyl)-2-(2,4,6-trinitrophenyl)hydrazine
• CAS No.: 4310-36-5
• Molecular Formula: C₁₈H₁₁Br₂N₅O₆
• Molecular Weight: 553.123
• DSSTox Substance ID: DTXSID901201317
• Nikkaji Number: J960.376J
• Mol file: 4310-36-5.mol

Synonyms:DTXSID901201317;4310-36-5;1,1-Bis(4-bromophenyl)-2-(2,4,6-trinitrophenyl)hydrazine

Chemical Property of 1,1-Bis(4-bromophenyl)-2-(2,4,6-trinitrophenyl)hydrazine

Chemical Property:

• XLogP3: 6.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 4
• Exact Mass: 552.90556
• Heavy Atom Count: 31
• Complexity: 609

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1N(C2=CC=C(C=C2)Br)NC3=C(C=C(C=C3[N+](=O)[O-])[N+](=O)[O-])[N+](=O)[O-])Br

Technology Process of 1,1-Bis(4-bromophenyl)-2-(2,4,6-trinitrophenyl)hydrazine

There total 5 articles about 1,1-Bis(4-bromophenyl)-2-(2,4,6-trinitrophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

2,2-diphenyl-1-(2,4,6-trinitrophenyl)hydrazyl (147506-92-1,1898-66-4) → 2-(p-bromophenyl)-2-phenyl-1-picrylhydrazine (4293-22-5) + 2-(p-bromophenyl)-2-phenyl-1-(2-bromo-4,6-dinitrophenyl)hydrazine (74852-56-5) + 2,2-diphenyl-1-picrylhydrazine (1707-75-1) + 1,1-Bis-<4-brom-phenyl>-2-pikryl-hydrazin (4310-36-5)

Guidance literature:

With bromine; In chloroform; at 0 - 2 ℃; for 1.5h; Further byproducts given;

Reference yield:

2,2-diphenyl-1-(2,4,6-trinitrophenyl)hydrazyl (147506-92-1,1898-66-4) → 2-(p-bromophenyl)-2-phenyl-1-picrylhydrazine (4293-22-5) + 2,2-diphenyl-1-picrylhydrazine (1707-75-1) + 2-(p-nitrophenyl)-2-phenyl-1-(2,4,6-trinitrophenyl)hydrazine (29946-26-7) + 1,1-Bis-<4-brom-phenyl>-2-pikryl-hydrazin (4310-36-5)

Guidance literature:

With bromine; In hexane; at 60 - 70 ℃; for 1.5h; Yield given. Further byproducts given;

Reference yield:

2,2-diphenyl-1-(2,4,6-trinitrophenyl)hydrazyl (147506-92-1,1898-66-4) → 2-(p-bromophenyl)-2-phenyl-1-picrylhydrazine (4293-22-5) + 2-(p-bromophenyl)-2-phenyl-1-(2-bromo-4,6-dinitrophenyl)hydrazine (74852-56-5) + 2-(p-nitrophenyl)-2-phenyl-1-(2,4,6-trinitrophenyl)hydrazine (29946-26-7) + 1,1-Bis-<4-brom-phenyl>-2-pikryl-hydrazin (4310-36-5)

Guidance literature:

With bromine; In chloroform; for 1.5h; Further byproducts given;

upstream raw materials:

2,2-diphenyl-1-(2,4,6-trinitrophenyl)hydrazyl