ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate

Base Information

Chemical Name:ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate
CAS No.:118191-08-5
Molecular Formula:C₁₅H₁₆ClN₃O₆
Molecular Weight:369.762
Hs Code.:

Synonyms:ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate

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Chemical Property of ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate

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Technology Process of ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate

There total 3 articles about ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 626-35-7
nitroacetic acid ethyl ester

: 118191-07-4
3-(dimethylamino)-2-(2-chloro-6-nitrophenyl)acrolein

: 118191-08-5
ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate

Guidance literature:: With acetic anhydride; at 80 - 90 ℃; for 0.75h;
DOI:10.1016/S0040-4039(00)86054-2

Reference yield:

: 83-42-1
6-chloro-2-nitrotoluene

: 118191-08-5
ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: 36 h / 110 - 120 °C

2: phosphorus oxychloride / 5.5 h / 25 °C

3: 92 percent / acetic anhydride / 0.75 h / 80 - 90 °C

With acetic anhydride; trichlorophosphate;
DOI:10.1016/S0040-4039(00)86054-2

Reference yield:

: 118191-06-3
2-chloro-6-nitrobenzaldehyde N,N-dimethylenamine

: 118191-08-5
ethyl 5-(dimethylamino)-2-nitro-4-(2-chloro-6-nitrophenyl)-2,4-pentadienoate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus oxychloride / 5.5 h / 25 °C

2: 92 percent / acetic anhydride / 0.75 h / 80 - 90 °C

With acetic anhydride; trichlorophosphate;
DOI:10.1016/S0040-4039(00)86054-2