Technology Process of C35H36O6
There total 13 articles about C35H36O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; methanol;
In
dichloromethane;
at 20 ℃;
-
-
4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: acetic anhydride; dimethyl sulfoxide / dimethyl sulfoxide / 20 °C / Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: -78 - 0 °C
2.3: cooling with ice
3.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C
4.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C
4.2: -78 - 0 °C
5.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C
6.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C
6.2: 0.75 h
7.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
7.2: 12 h / 40 °C
8.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
8.2: 2 h / 0 - 20 °C
9.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere
10.1: hydrogenchloride; methanol / dichloromethane / 20 °C
With
1H-imidazole; hydrogenchloride; methanol; sodium tetrahydroborate; n-butyllithium; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; acetic anhydride; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; trifluoroacetic anhydride;
18-crown-6 ether;
In
tetrahydrofuran; methanol; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 - 0 °C
1.3: cooling with ice
2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C
3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C
3.2: -78 - 0 °C
4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C
5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C
5.2: 0.75 h
6.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
6.2: 12 h / 40 °C
7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
7.2: 2 h / 0 - 20 °C
8.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere
9.1: hydrogenchloride; methanol / dichloromethane / 20 °C
With
1H-imidazole; hydrogenchloride; methanol; sodium tetrahydroborate; n-butyllithium; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; trifluoroacetic anhydride;
18-crown-6 ether;
In
tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;