4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol

Base Information

• Chemical Name: 4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol
• CAS No.: 643093-53-2
• Molecular Formula: C₂₃H₂₄ClNO₂
• Molecular Weight: 381.902

Synonyms:4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol

Chemical Property of 4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol

Chemical Property:

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Technology Process of 4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol

There total 1 articles about 4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-[[4-(2-{benzyl[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)-phenyl](hydroxy)methyl]phenol (643093-52-1) → 4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol (643093-53-2)

Guidance literature:

4-[[4-(2-{benzyl[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)-phenyl](hydroxy)methyl]phenol; With hydrogenchloride; In 1,4-dioxane; for 0.0833333h;

With hydrogen; palladium on activated charcoal; In ethanol; chlorobenzene; for 2h; Further stages.;

DOI:10.1021/jm701324c

Reference yield: 98.0%

4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol (643093-53-2) + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl (2R)-2-(3-chlorophenyl)-2-hydroxyethyl{2-[4-(4-hydroxybenzyl)phenyl]ethyl}carbamate (643093-54-3)

Guidance literature:

In tetrahydrofuran; water; at 20 ℃; for 0.5h;

DOI:10.1021/jm701324c

Reference yield:

4-[4-(2-{[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)benzyl]phenol (643093-53-2) + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl (2R)-N-[2-(3-chlorophenyl)-2-hydroxyethyl]-N-[2-[4-(4-hydroxybenzyl)phenyl]ethyl]carbamate

Guidance literature:

In tetrahydrofuran; water;

upstream raw materials:

4-[[4-(2-{benzyl[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino}ethyl)-phenyl](hydroxy)methyl]phenol

Downstream raw materials:

tert-butyl (2R)-2-(3-chlorophenyl)-2-hydroxyethyl{2-[4-(4-hydroxybenzyl)phenyl]ethyl}carbamate

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