2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone

Base Information

• Chemical Name: 2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone
• CAS No.: 132338-33-1
• Molecular Formula: C₁₂H₁₆N₂O₄
• Molecular Weight: 252.27

Synonyms:2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone

Chemical Property of 2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone

Chemical Property:

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Technology Process of 2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone

There total 1 articles about 2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-(2-hydroxy-4-methoxyphenyl)ethanone (552-41-0) + ethylhydrazine carboxylate (4114-31-2) → 2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone (132338-33-1)

Guidance literature:

With hydrogenchloride; In ethanol; at 80 ℃; for 2h;

DOI:10.3390/molecules22081348

Reference yield: 92.0%

2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone (132338-33-1) → 4-(2-hydroxy-4-methoxyphenyl)-1,2,3-thiadiazole

Guidance literature:

With thionyl chloride; In chloroform; N,N-dimethyl-formamide;

DOI:10.3390/molecules22081348

Reference yield: 76.0%

2-hydroxy-4-methoxyacetophenone ethoxycarbonylhydrazone (132338-33-1) → 2-Acetyl-5-methoxy-benzoic acid ethyl ester (132338-35-3)

Guidance literature:

With lead(IV) acetate; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1016/S0040-4039(00)97170-3

upstream raw materials:

1-(2-hydroxy-4-methoxyphenyl)ethanone

ethylhydrazine carboxylate

Downstream raw materials:

2-Acetyl-5-methoxy-benzoic acid ethyl ester

2-(4-Chloro-2-fluoro-5-hydroxy-phenyl)-6-methoxy-3-methylene-2,3-dihydro-isoindol-1-one

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