[8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate

Base Information

Chemical Name:[8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate
CAS No.:375385-76-5
Molecular Formula:C₂₅H₂₉NO₄
Molecular Weight:407.51
Hs Code.:

Synonyms:[8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate

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Chemical Property of [8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate

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Technology Process of [8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate

There total 3 articles about [8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (2E)-penta-2,4-dienyl pivalate

: 375385-70-9
N-(4,4-dimethoxy-2-methyl-cyclohexa-2,5-dienylidene)-benzamide

: 375385-76-5
[8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate

Guidance literature:: (2E)-penta-2,4-dienyl pivalate; N-(4,4-dimethoxy-2-methyl-cyclohexa-2,5-dienylidene)-benzamide; In dichloromethane; at 50 ℃; for 12h; under 9750780 Torr;

With hydrogenchloride; In tetrahydrofuran; for 0.0833333h;
DOI:10.1139/v03-188

Reference yield:

: 2,2-Dimethyl-propionic acid 8-[(E)-benzoylimino]-5,5-dimethoxy-7-methyl-1,4,4a,5,8,8a-hexahydro-naphthalen-1-ylmethyl ester

: 375385-76-5
[8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate

Guidance literature:: hydrogenchloride; In tetrahydrofuran; for 0.0833333h;
DOI:10.1021/ol016562k

Reference yield:

: 61495-08-7
N-(4-methoxy-2-methylphenyl)benzamide

: 375385-76-5
[8-(benzoylamino)-5-methoxy-7-methyl-1,4-dihydronaphthalen-1-yl]methyl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / LiClO₄ / NaHCO₃ / Electrochemical reaction

2.1: CH₂Cl₂ / 12 h / 50 °C / 9750780 Torr

2.2: 70 percent / aq. HCl / tetrahydrofuran / 0.08 h

With lithium perchlorate; sodium hydrogencarbonate; In dichloromethane; 2.1: Diels-Alder reaction;
DOI:10.1139/v03-188