3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one

Base Information

Chemical Name:3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one
CAS No.:1333248-36-4
Molecular Formula:C₂₇H₂₇N₃O₄
Molecular Weight:457.529
Hs Code.:

Synonyms:3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one

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Chemical Property of 3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one

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Technology Process of 3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one

There total 5 articles about 3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₀N₂O₅

: 94-70-2
ortho-phenitidine

: 1333248-36-4
3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one

Guidance literature:: With pyridine; triphenyl phosphite; at 230 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1016/j.bmcl.2011.07.043

Reference yield:

: 527-69-5
2-furancarbonyl chloride

: 1333248-36-4
3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

2: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C

3: pyridine; triphenyl phosphite / 0.17 h / 150 °C / Microwave irradiation

4: pyridine; triphenyl phosphite / 0.08 h / 230 °C / Microwave irradiation

With pyridine; triphenyl phosphite; water; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.07.043

Reference yield:

: 952934-82-6
C₁₃H₁₇NO₄

: 1333248-36-4
3-(2-ethoxyphenyl)-2-((1-(furan-2-carbonyl)piperidin-4-yl)methyl)quinazolin-4(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C

2: pyridine; triphenyl phosphite / 0.17 h / 150 °C / Microwave irradiation

3: pyridine; triphenyl phosphite / 0.08 h / 230 °C / Microwave irradiation

With pyridine; triphenyl phosphite; water; lithium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.07.043