2,3-dioxo-N-phenyl-1-indolinecarboxamide

Base Information

Chemical Name:2,3-dioxo-N-phenyl-1-indolinecarboxamide
CAS No.:53460-45-0
Molecular Formula:C₁₅H₁₀N₂O₃
Molecular Weight:266.256
Hs Code.:

Synonyms:2,3-dioxo-N-phenyl-1-indolinecarboxamide

Suppliers and Price of 2,3-dioxo-N-phenyl-1-indolinecarboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 2,3-dioxo-N-phenyl-1-indolinecarboxamide

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2,3-dioxo-N-phenyl-1-indolinecarboxamide

There total 4 articles about 2,3-dioxo-N-phenyl-1-indolinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 103-71-9
phenyl isocyanate

: 53460-45-0
2,3-dioxo-N-phenyl-1-indolinecarboxamide

Guidance literature:: With KF-Celite; In 2-methyltetrahydrofuran; for 12h; chemoselective reaction; Reflux;
DOI:10.1039/c5gc01002k

Reference yield:

: 42366-35-8,1769-41-1
hydroxyimino-N-phenylacetamide

: 53460-45-0
2,3-dioxo-N-phenyl-1-indolinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: conc. H₂SO₄ / Heating

2: Et₃N / dimethylformamide / 1 h / 0 °C

With sulfuric acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00089a021

Reference yield:

: 62-53-3
aniline

: 53460-45-0
2,3-dioxo-N-phenyl-1-indolinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂OH

2: conc. H₂SO₄ / Heating

3: Et₃N / dimethylformamide / 1 h / 0 °C

With sulfuric acid; hydroxylamine; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00089a021