Technology Process of C60H86N3O10PSi
There total 5 articles about C60H86N3O10PSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H33N2O4P; C50H68N2O5Si;
With
pyridinium trifluroacetate;
In
dichloromethane;
at -20 - -10 ℃;
With
dihydrogen peroxide;
In
dichloromethane; water;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
2.1: ethanol; water / 20 h / 20 °C
3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
4.1: ammonia; hydrogen / nickel / methanol / 20 h / 2585.81 Torr
5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C
6.1: pyridinium trifluroacetate / dichloromethane / -20 - -10 °C
6.2: 0.5 h / 20 °C
With
1H-imidazole; ammonia; hydrogen; pyridinium trifluroacetate; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid;
nickel;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonia; hydrogen / nickel / methanol / 20 h / 2585.81 Torr
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C
3.1: pyridinium trifluroacetate / dichloromethane / -20 - -10 °C
3.2: 0.5 h / 20 °C
With
ammonia; hydrogen; pyridinium trifluroacetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
nickel;
In
methanol; dichloromethane;
