Technology Process of inflachromene
There total 10 articles about inflachromene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; hydrogen fluoride;
In
tetrahydrofuran;
for 3h;
DOI:10.1039/b606341a
- Guidance literature:
-
4-Phenyl-1,2,4-triazolidine-3,5-dione; C22H34O2Si;
In
toluene;
at 20 ℃;
With
pyridine hydrogenfluoride;
In
tetrahydrofuran; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate; ethanol / 40 °C
1.2: 80 °C
1.3: 20 °C
2.1: trifluorormethanesulfonic acid / dichloromethane / 15 h / 0 - 20 °C
2.2: 2 h / 20 °C
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; water; toluene / 70 °C / Inert atmosphere
4.1: toluene / 0.5 h / 20 °C
5.1: pyridine; hydrogen fluoride / tetrahydrofuran
With
pyridine; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); ethanol; trifluorormethanesulfonic acid; hydrogen fluoride; sodium carbonate;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
3.1: Suzuki coupling / 4.1: Aza-Diels-Alder reaction;
DOI:10.1021/co2001907