4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose

Base Information

Chemical Name:4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose
CAS No.:399510-76-0
Molecular Formula:C₂₆H₄₈O₄Si₂
Molecular Weight:480.836
Hs Code.:

Synonyms:4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose

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Chemical Property of 4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose

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Technology Process of 4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose

There total 2 articles about 4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 274692-85-2
(1R,2R,3R,4R)-1,4-di-benzyloxy-2,3-(tert-butyldimethyl)silyloxy-5-methylenecyclohexane

: 274692-87-4
2,3-(tert-butyldimethyl)silyloxy-5a-carba-α-L-fucopyranose

: 399510-76-0
4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose

Guidance literature:: (1R,2R,3R,4R)-1,4-di-benzyloxy-2,3-(tert-butyldimethyl)silyloxy-5-methylenecyclohexane; With hydrogen; palladium on activated charcoal; In pyridine; methanol; at 20 ℃; for 2h;

With hydrogen; ammonium formate; palladium on activated charcoal; In methanol; at 70 ℃; for 4h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6

Reference yield: 18.0%

: 274692-85-2
(1R,2R,3R,4R)-1,4-di-benzyloxy-2,3-(tert-butyldimethyl)silyloxy-5-methylenecyclohexane

: 274692-87-4
2,3-(tert-butyldimethyl)silyloxy-5a-carba-α-L-fucopyranose

: 399510-76-0
4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose

: C₃₃H₅₄O₄Si₂

Guidance literature:: With hydrogen; ammonium formate; palladium on activated charcoal; In methanol; at 70 ℃; for 6h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6

Reference yield: 98.0%

: 399510-76-0
4-O-benzyl-2,3-di-O-(tert-butyldimethyl)silyl-5a-carba-α-L-fucopyranose

: 399510-94-2
4-O-benzyl-5a-carba-α-L-fucopyranose

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6