(η(6)-p-cymene)OsCl2(PPh3)

Base Information

Chemical Name:(η(6)-p-cymene)OsCl2(PPh3)
CAS No.:96390-95-3
Molecular Formula:C₂₈H₂₉Cl₂OsP
Molecular Weight:657.618
Hs Code.:

Synonyms:(η(6)-p-cymene)OsCl2(PPh3)

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Chemical Property of (η(6)-p-cymene)OsCl2(PPh3)

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Technology Process of (η(6)-p-cymene)OsCl2(PPh3)

There total 4 articles about (η(6)-p-cymene)OsCl2(PPh3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: [osmium(II)dichloride(η6-p-cymene)]2

: 96390-95-3
(η(6)-p-cymene)OsCl2(PPh3)

Guidance literature:: With triphenylphosphine; In dichloromethane; PPh3 added to soln. of ((p-MeC6H4CHMe2)2Os2Cl4) in CH2Cl2; hexane added, suspn. vac.-concd., Et2O added, crystals filtered off andwashed with Et2O; elem. anal.;
DOI:10.1039/DT9850000573

Reference yield: 92.0%

: 2Os⁽²⁺⁾*4Cl^(1-)*C₆H₄(CH₃)CH(CH₃)2 = Os₂(C₆H₄(CH₃)CH(CH₃)2)Cl₄

: 96390-95-3
(η(6)-p-cymene)OsCl2(PPh3)

Guidance literature:: With triphenylphosphine; elem. anal.;
DOI:10.1039/c39850000065

Reference yield: 76.0%

: bis[dichlorido(η6-p-cymene)osmium(II)]

: 603-35-0
triphenylphosphine

: 96390-95-3
(η(6)-p-cymene)OsCl2(PPh3)

Guidance literature:: In dichloromethane; addn. of PPh3 (1.5 mmol) to {(p-Cym)OsCl2}2 soln. (0.5 mmol;CH2Cl2), stirring, 40 °C, 3h, cooling, dried, soln. of residue in CH2Cl2, filtration, washing of residue with CH2Cl2 several times, concn. of filtrates, addn. of hexane, pptn.; all in N2; washing several times (hexane), drying under vac.; all operations under purified N2, solvents carefully dried, elem. anal.;
DOI:10.1016/0022-328X(88)80244-4