5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

Base Information

Chemical Name:5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester
CAS No.:165196-55-4
Molecular Formula:C₂₈H₂₈O₅S₈Si
Molecular Weight:729.141
Hs Code.:

Synonyms:5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

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Chemical Property of 5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

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Technology Process of 5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

There total 1 articles about 5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 68128-93-8
4-(hydroxymethyl)tetrathiafulvalene

: 5-(tert-butyldimethylsiloxy)-isophthaloyl dichloride

: 165196-55-4
5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h;

Reference yield: 85.0%

: 165196-55-4
5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

: 165196-56-5
5-Hydroxy-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield:

: 165196-55-4
5-(tert-Butyl-dimethyl-silanyloxy)-isophthalic acid di[2,2']bi[[1,3]dithiolylidene]-4-ylmethyl ester

: Biphenyl-4,4'-dicarboxylic acid bis-[3,5-bis-([2,2']bi[[1,3]dithiolylidene]-4-ylmethoxycarbonyl)-phenyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 18 h / 20 °C

2: 83 percent / DMAP / CH₂Cl₂ / 18 h / 20 °C

With dmap; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/a800225h