C₆₁H₇₀O₁₆

Base Information

Chemical Name:C₆₁H₇₀O₁₆
CAS No.:77735-10-5
Molecular Formula:C₆₁H₇₀O₁₆
Molecular Weight:1059.22
Hs Code.:

C<sub>61</sub>H<sub>70</sub>O<sub>16</sub>

Synonyms:C₆₁H₇₀O₁₆

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Chemical Property of C₆₁H₇₀O₁₆

Chemical Property:

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Technology Process of C₆₁H₇₀O₁₆

There total 9 articles about C₆₁H₇₀O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 77735-06-9
methyl 2-O-benzoyl-6-O-(2-O-benzoyl-3,4-di-O-benzyl-β-D-galactopyranosyl)-3,4-di-O-benzyl-β-D-galactopyranoside

: 77735-10-5
C₆₁H₇₀O₁₆

Guidance literature:: With sodium methylate; In methanol; Ambient temperature;
DOI:10.1016/S0008-6215(00)85899-1

Reference yield:

: 66963-43-7
1,6-anhydro-3,4-di-O-benzyl-β-D-galactopyranose

: 77735-10-5
C₆₁H₇₀O₁₆

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / triethylamine / 1 h / Ambient temperature

2: 97 percent / concd. H₂SO₄ / acetic acid / 8 h / 10 °C

3: 76 percent / HCl / diethyl ether / 48 h / Ambient temperature

4: 1.) silver p-toluenesulfonate / 1.) methanol; 2.) room temp., 17 h, acetonitrile

5: 84 percent / ammonium hydroxide (32percent) / methanol / Ambient temperature

6: 89 percent / sodium methoxide / methanol / Ambient temperature

With hydrogenchloride; ammonium hydroxide; sulfuric acid; sodium methylate; silver(I) 4-methylbenzenesulfonate; In methanol; diethyl ether; acetic acid; triethylamine;
DOI:10.1016/S0008-6215(00)85899-1

Reference yield:

: 100-44-7
benzyl chloride

: 77735-10-5
C₆₁H₇₀O₁₆

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) sodium hydride / 1.) THF; 2.) reflux, 36 h

2: 93 percent / potassium tert-butoxide / toluene / 17 h / Heating

3: 56 percent / HCl (5percent) / dioxane / Heating

4: 85 percent / triethylamine / 1 h / Ambient temperature

5: 97 percent / concd. H₂SO₄ / acetic acid / 8 h / 10 °C

6: 76 percent / HCl / diethyl ether / 48 h / Ambient temperature

7: 1.) silver p-toluenesulfonate / 1.) methanol; 2.) room temp., 17 h, acetonitrile

8: 84 percent / ammonium hydroxide (32percent) / methanol / Ambient temperature

9: 89 percent / sodium methoxide / methanol / Ambient temperature

With hydrogenchloride; ammonium hydroxide; sulfuric acid; potassium tert-butylate; sodium methylate; silver(I) 4-methylbenzenesulfonate; sodium hydride; In 1,4-dioxane; methanol; diethyl ether; acetic acid; triethylamine; toluene;
DOI:10.1016/S0008-6215(00)85899-1