C₂₃H₂₃Cl₂P

Base Information

Chemical Name:C₂₃H₂₃Cl₂P
CAS No.:1417444-15-5
Molecular Formula:C₂₃H₂₃Cl₂P
Molecular Weight:401.315
Hs Code.:

C<sub>23</sub>H<sub>23</sub>Cl<sub>2</sub>P

Synonyms:C₂₃H₂₃Cl₂P

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Chemical Property of C₂₃H₂₃Cl₂P

Chemical Property:

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Technology Process of C₂₃H₂₃Cl₂P

There total 5 articles about C₂₃H₂₃Cl₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1417444-13-3
C₂₃H₂₃Cl₂OP

: 1417444-15-5
C₂₃H₂₃Cl₂P

Guidance literature:: With trichlorosilane; N-ethyl-N,N-diisopropylamine; In toluene; at 0 - 110 ℃; for 12h;
DOI:10.1021/ja312125a

Reference yield:

: 33974-41-3
neopentylmagnesium bromide

: 1417444-15-5
C₂₃H₂₃Cl₂P

Guidance literature:: Multi-step reaction with 5 steps

1: [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride / diethyl ether / 8 h / 0 °C / Inert atmosphere; Reflux

2: boron tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

4: N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; palladium diacetate / dimethyl sulfoxide / 8 h / 100 °C / Inert atmosphere

5: N-ethyl-N,N-diisopropylamine; trichlorosilane / toluene / 12 h / 0 - 110 °C

With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; trichlorosilane; palladium diacetate; boron tribromide; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/ja312125a

Reference yield:

: 578-57-4
2-bromoanisole

: 1417444-15-5
C₂₃H₂₃Cl₂P

Guidance literature:: Multi-step reaction with 5 steps

1: [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride / diethyl ether / 8 h / 0 °C / Inert atmosphere; Reflux

2: boron tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

4: N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; palladium diacetate / dimethyl sulfoxide / 8 h / 100 °C / Inert atmosphere

5: N-ethyl-N,N-diisopropylamine; trichlorosilane / toluene / 12 h / 0 - 110 °C

With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; trichlorosilane; palladium diacetate; boron tribromide; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/ja312125a