Technology Process of C31H31F2N3O5
There total 18 articles about C31H31F2N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; ammonium formate;
In
acetone;
for 12h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diethylamino-sulfur trifluoride / toluene / 0.5 h / -78 - 60 °C
2.1: water / acetonitrile / 20 °C
3.1: Triphenylsilyl chloride; dmap; triethylamine / acetonitrile / 20 °C
3.2: 2 h
3.3: 20 °C
4.1: palladium 10% on activated carbon; ammonium formate / acetone / 12 h / Reflux
With
dmap; Triphenylsilyl chloride; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; water; ammonium formate; triethylamine;
In
acetone; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: water / acetonitrile / 20 °C
2.1: Triphenylsilyl chloride; dmap; triethylamine / acetonitrile / 20 °C
2.2: 2 h
2.3: 20 °C
3.1: palladium 10% on activated carbon; ammonium formate / acetone / 12 h / Reflux
With
dmap; Triphenylsilyl chloride; palladium 10% on activated carbon; water; ammonium formate; triethylamine;
In
acetone; acetonitrile;