8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Base Information

• Chemical Name: 8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine
• CAS No.: 41282-12-6
• Molecular Formula: C₁₈H₁₃Cl₂N₃
• Molecular Weight: 342.227

Synonyms:8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Chemical Property of 8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Chemical Property:

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Technology Process of 8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

There total 2 articles about 8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

3-amino-2-propanol (78-96-6,1674-56-2) + 7-chloro-5-(2-chlorophenyl)-2-(N-nitrosomethylamino)-3H-1,4-benzodiazepine (59467-72-0) → 8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine (41282-12-6)

Guidance literature:

3-amino-2-propanol; 7-chloro-5-(2-chlorophenyl)-2-(N-nitrosomethylamino)-3H-1,4-benzodiazepine; at 20 ℃; for 24h;

With jones' reagent; In acetone; at 20 ℃; for 1h;

With toluene-4-sulfonic acid; In toluene; at 80 ℃; for 14h;

DOI:10.3390/11080583

Reference yield:

mercury(II) sulfate + [7-chloro-5-(2-chloro-phenyl)-3H-benzo[e][1,4]diazepin-2-yl]-prop-2-ynyl-amine (41282-04-6) → 8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine (41282-12-6)

Guidance literature:

With sodium hydroxide; sulfuric acid;

Reference yield:

8-chloro-6-(2-chloro-phenyl)-1-methyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine (41282-12-6) → 8-chloro-6-(2-chlorophenyl)-1-methyl-4H-imidazo[1,2-a][1,4]benzodiazepine-5-oxide (41282-29-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In ethanol; potassium carbonate;

upstream raw materials:

3-amino-2-propanol

7-chloro-5-(2-chlorophenyl)-2-(N-nitrosomethylamino)-3H-1,4-benzodiazepine

[7-chloro-5-(2-chloro-phenyl)-3H-benzo[e][1,4]diazepin-2-yl]-prop-2-ynyl-amine

Downstream raw materials:

8-chloro-6-(2-chlorophenyl)-1-methyl-4H-imidazo[1,2-a][1,4]benzodiazepine-5-oxide

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