3-nitro-benzoic acid o-toluidide

Base Information Edit

Chemical Name:3-nitro-benzoic acid o-toluidide
CAS No.:102631-02-7
Molecular Formula:C₁₄H₁₂N₂O₃
Molecular Weight:256.261
Hs Code.:
Mol file:102631-02-7.mol

Synonyms:3-nitro-benzoic acid o-toluidide

Suppliers and Price of 3-nitro-benzoic acid o-toluidide

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 3-nitro-benzoic acid o-toluidide Edit

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of 3-nitro-benzoic acid o-toluidide

There total 2 articles about 3-nitro-benzoic acid o-toluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 95-53-4
o-toluidine

: 121-90-4
m-nitrobenzoic acid chloride

: 102631-02-7
3-nitro-benzoic acid o-toluidide

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/jm00158a038

Reference yield:

: 121-92-6
3-nitrobenzoic acid

: 102631-02-7
3-nitro-benzoic acid o-toluidide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: Na₂CO₃ / diethyl ether

With thionyl chloride; sodium carbonate; In diethyl ether;
DOI:10.1039/b210106h