C₃₂H₃₆O₅Si

Base Information

Chemical Name:C₃₂H₃₆O₅Si
CAS No.:1360932-96-2
Molecular Formula:C₃₂H₃₆O₅Si
Molecular Weight:528.72
Hs Code.:

C<sub>32</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:C₃₂H₃₆O₅Si

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Chemical Property of C₃₂H₃₆O₅Si

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Technology Process of C₃₂H₃₆O₅Si

There total 9 articles about C₃₂H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₃₄H₄₂O₆Si

: 1360932-96-2
C₃₂H₃₆O₅Si

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 16h; Reflux;
DOI:10.1002/chem.201102192

Reference yield:

: 705-76-0
3,5-dimethoxybenzyl alcohol

: 1360932-96-2
C₃₂H₃₆O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 1 h / 0 °C

2.2: 3 h / 20 °C

3.1: aluminum (III) chloride; sodium iodide / dichloromethane; acetonitrile / 1 h / 0 °C

4.1: (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid / toluene / 88 h / 20 °C

5.1: triethylamine / tetrahydrofuran / 0 - 20 °C

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 96 h / 20 °C

7.1: toluene / 100 °C

8.1: 5% Pd-BaSO4; hydrogen / ethyl acetate / 1 h / 20 °C / 750.08 Torr

9.1: toluene-4-sulfonic acid / tetrahydrofuran / 24 h / 20 °C

10.1: toluene-4-sulfonic acid / benzene / 16 h / Reflux

With 1H-imidazole; aluminum (III) chloride; osmium(VIII) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; 5% Pd-BaSO4; hydrogen; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; benzoic acid; sodium iodide; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; benzene; 7.1: Wittig reaction;
DOI:10.1002/chem.201102192

Reference yield:

: 1132-21-4
3,5-dimethoxybenzoic acid

: 1360932-96-2
C₃₂H₃₆O₅Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 1 h / 0 °C

3.2: 3 h / 20 °C

4.1: aluminum (III) chloride; sodium iodide / dichloromethane; acetonitrile / 1 h / 0 °C

5.1: (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; benzoic acid / toluene / 88 h / 20 °C

6.1: triethylamine / tetrahydrofuran / 0 - 20 °C

7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 96 h / 20 °C

8.1: toluene / 100 °C

9.1: 5% Pd-BaSO4; hydrogen / ethyl acetate / 1 h / 20 °C / 750.08 Torr

10.1: toluene-4-sulfonic acid / tetrahydrofuran / 24 h / 20 °C

11.1: toluene-4-sulfonic acid / benzene / 16 h / Reflux

With 1H-imidazole; aluminum (III) chloride; osmium(VIII) oxide; lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; 5% Pd-BaSO4; hydrogen; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; benzoic acid; sodium iodide; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; benzene; 8.1: Wittig reaction;
DOI:10.1002/chem.201102192