1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl

Base Information

• Chemical Name: 1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl
• CAS No.: 625111-44-6
• Molecular Formula: C₂₀H₂₁N₅O₉S₂
• Molecular Weight: 539.547

Synonyms:1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl

Chemical Property of 1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl

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Technology Process of 1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl

There total 1 articles about 1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

9-(3-O-benzyl-5-O-(methanesulfonyl)-4-C-[[(methanesulfonyl)oxy]methyl]-2-O-trifluoromethanesulfonyl-α-L-threo-pentofuranosyl)-6-N-benzoyladenine → 1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl (625111-44-6)

Guidance literature:

With methanesulfonic acid; In dichloromethane; at 20 ℃;

Reference yield: 80.0%

1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl (625111-44-6) → 9-(2-azido-3-O-benzyl-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-threo-pentofuranosyl)-6-N-benzoyladenine (625111-46-8)

Guidance literature:

With sodium azide; In DMF (N,N-dimethyl-formamide); at 50 ℃;

Reference yield: 30.0%

1-(2',3'-epoxide-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-erythro-pentofuranosyl)-6-benzoyl adenine-9-yl (625111-44-6) → (1R,3R,4R,7S)-7-hydroxy-1-methanesulfonyloxymethyl-3-(6-benzoyladenin-9-yl)-2-oxa-5-thiabicyclo[2.2.1]heptane

Guidance literature:

With sodium sulfide; In DMF (N,N-dimethyl-formamide); at 20 ℃;

Downstream raw materials:

9-(2-azido-3-O-benzyl-4-C-methanesulfonyloxymethyl-5-O-methanesulfonyl-2-deoxy-α-L-threo-pentofuranosyl)-6-N-benzoyladenine

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