triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane

Base Information

Chemical Name:triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane
CAS No.:1357111-42-2
Molecular Formula:C₂₉H₄₄O₄Si
Molecular Weight:484.751
Hs Code.:

Synonyms:triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane

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Chemical Property of triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane

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Technology Process of triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane

There total 4 articles about triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1357111-41-1
2-(4-methoxybenzyloxy)butyric acid 1-phenylethyl ester

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1357111-42-2
triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane

Guidance literature:: 2-(4-methoxybenzyloxy)butyric acid 1-phenylethyl ester; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h; Inert atmosphere;

triisopropylsilyl trifluoromethanesulfonate; In tetrahydrofuran; toluene; at -78 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.12.011

Reference yield:

: 1157983-47-5
2-(4-(methoxy)benzyloxy)butyric acid

: 1357111-42-2
triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 1 h / 0 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 0 °C / Inert atmosphere

With dmap; 2,4,6-trichlorobenzoyl chloride; potassium hexamethylsilazane; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/j.tetlet.2011.12.011

Reference yield:

: 1357111-37-5
2-(4-methoxybenzyloxy)butyric acid ethyl ester

: 1357111-42-2
triisopropyl-[2-(4-methoxybenzyloxy)-1-(1-phenylethoxy)but-1-enyloxy]silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hydroxide / tetrahydrofuran; water / 16.5 h / 0 - 20 °C

1.2: pH 4

2.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 1 h / 0 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 - 0 °C / Inert atmosphere

With dmap; 2,4,6-trichlorobenzoyl chloride; potassium hexamethylsilazane; triethylamine; lithium hydroxide; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.tetlet.2011.12.011