N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester

Base Information

Chemical Name:N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester
CAS No.:331821-49-9
Molecular Formula:C₃₀H₄₆N₄O₇S₂
Molecular Weight:638.85
Hs Code.:

Synonyms:N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester

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Chemical Property of N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester

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Technology Process of N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester

There total 3 articles about N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40290-63-9
Methyl ester of N-t-butyloxycarbonyl-L-phenylalanyl-L-methionine

: 331821-49-9
N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / dioxane / 0.08 h / Heating

2: 67 percent / Et₃N; HOBt; EDC / dimethylformamide / -10 - 20 °C

With hydrogenchloride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jo001257i

Reference yield:

: 120711-54-8
L-(-)-N-(tert-butyloxycarbonyl)-2,2-dimethylthiazolidinecarboxylic acid pentafluorophenyl ester

: 331821-49-9
N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N / tetrahydrofuran / 23 h / 20 °C

2: 94 percent / aq. NaOH / ethanol / 24 h / 20 °C

3: 67 percent / Et₃N; HOBt; EDC / dimethylformamide / -10 - 20 °C

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo001257i

Reference yield:

: 331821-82-0
N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycine methyl ester

: 331821-49-9
N-Boc-L-2,2-dimethylthiazolidine-4-carbonyl-L-ethylglycyl-L-phenylalanyl-L-methionine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. NaOH / ethanol / 24 h / 20 °C

2: 67 percent / Et₃N; HOBt; EDC / dimethylformamide / -10 - 20 °C

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo001257i