(3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

Base Information

Chemical Name:(3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate
CAS No.:1172139-87-5
Molecular Formula:C₁₅H₁₉NO₄
Molecular Weight:277.32
Hs Code.:

Synonyms:(3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

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Chemical Property of (3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

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Technology Process of (3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

There total 3 articles about (3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.7%

: 1172140-02-1
benzyl (R)-2-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl carbamate

: 1172139-87-5
(3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

Guidance literature:: benzyl (R)-2-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl carbamate; With Oxone; 1,1,1-trifluoro-2-propanone; edetate disodium; sodium hydrogencarbonate; In water; acetonitrile; at 0 ℃; for 1.66667h;

With sodium hydride; In tetrahydrofuran; paraffin oil (nujol); at 20 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: C₁₅H₁₉NO₄

: 1172139-87-5
(3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

Guidance literature:: C₁₅H₁₉NO₄; With sodium hydride; In tetrahydrofuran; paraffin oil (nujol); at 20 ℃; Inert atmosphere;

With water; In tetrahydrofuran; paraffin oil (nujol); dichloromethane;

Reference yield:

: 1172140-05-4
(3R,3aR,6R,6aR)-6-methylhexahydro-2H-furo[3,2-b]pyrrol-3-ol

: 501-53-1,94274-21-2
benzyl chloroformate

: 1172139-87-5
(3R,3aR,6R,6aR)-benzyl 3-hydroxy-6-methyltetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

Guidance literature:: (3R,3aR,6R,6aR)-6-methylhexahydro-2H-furo[3,2-b]pyrrol-3-ol; With sodium carbonate; In tetrahydrofuran; diethyl ether; water; for 0.416667h;

benzyl chloroformate; In tetrahydrofuran; diethyl ether; water; for 1.83333h;