(E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate

Base Information

Chemical Name:(E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate
CAS No.:359418-00-1
Molecular Formula:C₁₆H₉F₁₃O₂
Molecular Weight:480.225
Hs Code.:

Synonyms:(E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate

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Chemical Property of (E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate

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Technology Process of (E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate

There total 4 articles about (E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 619-42-1
4-methoxycarbonylphenyl bromide

: 25291-17-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene

: 359418-00-1
(E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate

Guidance literature:: With sodium acetate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); In N,N-dimethyl-formamide; at 125 ℃; for 10h;
DOI:10.1016/S0040-4039(01)00714-6

Reference yield: 93.0%

: 25291-17-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene

: 619-44-3
methyl 4-iodobenzoate

: 359418-00-1
(E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate

Guidance literature:: With tetrabutylammomium bromide; sodium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 110 ℃; for 24h;
DOI:10.1016/S0040-4039(01)00714-6

Reference yield: 55.0%

: 335-56-8
1-bromo-1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluorohexane

: 1076-96-6
methyl 4-vinylbenzoate

: 359418-00-1
(E)-methyl 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-en-1-yl)benzoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,2-dichloro-ethane; at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201409617