isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide

Base Information

Chemical Name:isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide
CAS No.:1302580-00-2
Molecular Formula:C₁₉H₂₁N₃O₃S
Molecular Weight:371.46
Hs Code.:

Synonyms:isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide

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Chemical Property of isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide

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Technology Process of isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide

There total 2 articles about isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1302579-22-1
(S)-2,2-dimethyl-4-[(E)-2-(4-nitrophenyl)vinyl]oxazolidine-3-carboxylic acid tert-butyl ester

: 1302580-00-2
isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium formate / palladium 10% on activated carbon / methanol / 2 h / 6 °C

2.1: triethylamine / tetrahydrofuran / 20 - 50 °C

3.1: trifluoroacetic acid / acetonitrile; water / 5 h / 20 - 50 °C

3.2: pH 14

With ammonium formate; triethylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; water; acetonitrile;

Reference yield:

: (S)-4-[2-(4-amino-phenyl)-ethyl]-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 1302580-00-2
isoquinoline-5-sulfonic acid [4-((S)-3-amino-4-hydroxy-butyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 20 - 50 °C

2.1: trifluoroacetic acid / acetonitrile; water / 5 h / 20 - 50 °C

2.2: pH 14

With triethylamine; trifluoroacetic acid; In tetrahydrofuran; water; acetonitrile;