erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

Base Information

Chemical Name:erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester
CAS No.:108379-13-1
Molecular Formula:C₂₂H₂₃N₃O₇S
Molecular Weight:473.507
Hs Code.:

erythro-N<sup>α</sup>-benzyloxycarbonyl-β-hydroxy-N<sup>im(τ)</sup>-tosyl-L-histidine methyl ester

Synonyms:erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

Suppliers and Price of erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

There total 4 articles about erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-59-9
p-toluenesulfonyl chloride

: 141243-31-4
N^α-((benzyloxy)carbonyl)-erythro-β-hydroxy-L-histidine methyl ester

: 108379-13-1
erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

Guidance literature:: With sodium carbonate; In 1,4-dioxane; water; 0 deg C, 30 min then roomtemp., 2 h;
DOI:10.1246/bcsj.59.1387

Reference yield:

: 41215-80-9
erythro-β-hydroxy-L-histidine hydrate

: 108379-13-1
erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / triethylamine / H₂O; dioxane / 2.5 h / Ambient temperature

2: 78 percent / 10percent HCl / 7 h / 40 °C

3: 98 percent / sodium carbonate / dioxane; H₂O / 0 deg C, 30 min then roomtemp., 2 h

With hydrogenchloride; sodium carbonate; triethylamine; In 1,4-dioxane; water;
DOI:10.1246/bcsj.59.1387

Reference yield:

: 101485-34-1
N^α-(benzyloxycarbonyl)-erythro-β-hydroxy-L-histidine

: 108379-13-1
erythro-N^α-benzyloxycarbonyl-β-hydroxy-N^im(τ)-tosyl-L-histidine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 10percent HCl / 7 h / 40 °C

2: 98 percent / sodium carbonate / dioxane; H₂O / 0 deg C, 30 min then roomtemp., 2 h

With hydrogenchloride; sodium carbonate; In 1,4-dioxane; water;
DOI:10.1246/bcsj.59.1387