(E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate

Base Information

Chemical Name:(E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate
CAS No.:1572184-26-9
Molecular Formula:C₃₃H₃₆N₄O₅
Molecular Weight:568.673
Hs Code.:

Synonyms:(E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate

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Chemical Property of (E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate

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Technology Process of (E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate

There total 7 articles about (E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 110-91-8,99108-56-2
morpholine

: 626-16-4
3-(chloromethyl)benzyl chloride

: 1572184-13-4
(E)-N’-((1H-indol-6-yl)methylene)-N-(hydroxymethyl)-2-(mesityloxy)acetohydrazide

: 1572184-26-9
(E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate

Guidance literature:: 3-(chloromethyl)benzyl chloride; (E)-N’-((1H-indol-6-yl)methylene)-N-(hydroxymethyl)-2-(mesityloxy)acetohydrazide; With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

morpholine; With sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield: 32.0%

: 110-91-8,99108-56-2
morpholine

: 626-16-4
3-(chloromethyl)benzyl chloride

: 1572184-19-0
(E)-N’-((1H-indol-4-yl)methylene)-N-(hydroxymethyl)-2-(mesityloxy)acetohydrazide

: 1572184-26-9
(E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate

Guidance literature:: 3-(chloromethyl)benzyl chloride; (E)-N’-((1H-indol-4-yl)methylene)-N-(hydroxymethyl)-2-(mesityloxy)acetohydrazide; With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

morpholine; With sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 527-60-6
Mesitol

: 1572184-26-9
(E)-(2-((1H-indol-6-yl)methylene)-1-(2-(mesityloxy)acetyl)hydrazinyl)methyl4-(morpholinomethyl)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

2.1: tetrahydrofuran / 1 h / 20 °C

3.1: ethanol / 3 h / 90 °C

4.1: potassium carbonate; formaldehyd / N,N-dimethyl-formamide / 48 h / 40 °C

5.1: pyridine / N,N-dimethyl-formamide / 3 h / 20 °C

5.2: 4 h / 20 °C

With pyridine; formaldehyd; potassium carbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;