Technology Process of C54H32N2O2
There total 2 articles about C54H32N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water; toluene;
for 8h;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; 1,2-dimethoxyethane; water / 8 h / Reflux; Inert atmosphere
2: N-Bromosuccinimide / N,N-dimethyl-formamide / 8 h / 20 °C / Inert atmosphere
3: boron tribromide / dichloromethane / 8 h / 0 °C / Inert atmosphere
4: potassium carbonate / 1-methyl-pyrrolidin-2-one / 8 h / 150 °C / Inert atmosphere
5: potassium phosphate; trans-1,2-cyclohexanediamine / copper(l) iodide / 1,4-dioxane / 10 h / Inert atmosphere; Reflux
6: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; 1,2-dimethoxyethane; water / 8 h / Reflux; Inert atmosphere
With
potassium phosphate; N-Bromosuccinimide; boron tribromide; sodium carbonate; potassium carbonate; trans-1,2-cyclohexanediamine;
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; 1-methyl-pyrrolidin-2-one; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;