2-fluoro-4-nitrophenylsulfur pentafluoride

Base Information

Chemical Name:2-fluoro-4-nitrophenylsulfur pentafluoride
CAS No.:864230-04-6
Molecular Formula:C₆H₃F₆NO₂S
Molecular Weight:267.152
Hs Code.:

Synonyms:2-fluoro-4-nitrophenylsulfur pentafluoride

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Chemical Property of 2-fluoro-4-nitrophenylsulfur pentafluoride

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Technology Process of 2-fluoro-4-nitrophenylsulfur pentafluoride

There total 4 articles about 2-fluoro-4-nitrophenylsulfur pentafluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: C₆H₃ClF₅NO₂S

: 864230-04-6
2-fluoro-4-nitrophenylsulfur pentafluoride

Guidance literature:: With silver carbonate; at 100 ℃; for 60h; Inert atmosphere; Glovebox;
DOI:10.1039/c7cc07222h

Reference yield:

: 1,2-bis(2-fluoro-4-nitrophenyl)disulfane

: 864230-04-6
2-fluoro-4-nitrophenylsulfur pentafluoride

Guidance literature:: With fluorine; In acetonitrile; at -3 - 0 ℃; for 32h;
DOI:10.1002/ejoc.200500125

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 864230-04-6
2-fluoro-4-nitrophenylsulfur pentafluoride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium sulfide / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / water / 0.5 h / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

3.1: potassium fluoride; chlorine / acetonitrile / 20 °C / Inert atmosphere; Glovebox; Cooling with ice

4.1: silver carbonate / 60 h / 100 °C / Inert atmosphere; Glovebox

With sodium sulfide; potassium fluoride; chlorine; silver carbonate; sodium hydroxide; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c7cc07222h