4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline

Base Information

Chemical Name:4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline
CAS No.:1421755-98-7
Molecular Formula:C₃₄H₄₁NS₃
Molecular Weight:559.904
Hs Code.:

Synonyms:4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline

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Chemical Property of 4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline

Chemical Property:

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Technology Process of 4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline

There total 4 articles about 4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1354780-55-4
4-bromo-N,N-bis(4-(hexylthio)phenyl)aniline

: 193978-23-3
2-thiopheneboronic acid pinacol ester

: 1421755-98-7
4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; for 16h; Inert atmosphere; Reflux;
DOI:10.1021/ja311640f

Reference yield:

: 81090-53-1
N,N-bis(4-bromophenyl)aniline

: 1421755-98-7
4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 2 h

1.2: 18 h / Reflux

2.1: N-Bromosuccinimide / ethyl acetate / 24 h / 25 °C / Darkness

3.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 16 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; sodium carbonate; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1021/ja311640f

Reference yield:

: 1354780-54-3
C₃₀H₃₉NS₂

: 1421755-98-7
4-(hexylthio)-N-(4-(hexylthio)phenyl)-N-(4-(thiophen-2-yl)phenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / ethyl acetate / 24 h / 25 °C / Darkness

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 16 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1021/ja311640f