3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran

Base Information

Chemical Name:3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran
CAS No.:1357077-15-6
Molecular Formula:C₁₆H₂₀O₄
Molecular Weight:276.332
Hs Code.:

Synonyms:3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran

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Chemical Property of 3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran

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Technology Process of 3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran

There total 1 articles about 3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 1357077-18-9
3-acetyl-3-benzylheptane-2,6-dione

: 1357077-15-6
3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran

: 4-(7-benzyl-1,4-dimethyl-2,3,5,6-tetraoxabicyclo-[2.2.1]heptan-7-yl)butan-2-one

: 1-[(1R,2R,5S)-2-benzyl-1,5-dimethyl-6,7,8-trioxabicyclo[3.2.1]octan-2-yl]ethanone

: 1-[(1R,2S,5S)-2-benzyl-1,5-dimethyl-6,7,8-trioxabicyclo[3.2.1]octan-2-yl]ethanone

Guidance literature:: With phosphomolybdic acid; dihydrogen peroxide; In diethyl ether; toluene; at 20 - 25 ℃; for 8h; Reagent/catalyst; Solvent; Green chemistry;
DOI:10.1134/S1070428015120027

Reference yield:

: 1357077-15-6
3a-benzyl-3,6,7a-trimethyltetrahydro-3H,4H-3,6-epoxy[1,2]-dioxolo[3,4-b]pyran

: 1-(5-hydroxy-5-methyl-2-(phenylmethyl)tetrahydro-2-furanyl)ethanone

: 3-benzyl-3-hydroxyheptane-2,6-dione

Guidance literature:: With ferrous(II) sulfate heptahydrate; sulfuric acid; In water; acetonitrile; at 20 - 25 ℃; for 1h; Reagent/catalyst; Time; Overall yield = 92 %; Overall yield = 234 mg;
DOI:10.1016/j.tet.2016.04.054